Izithasiselo ze-nickel zokushisa okuphezulu

Izithasiselo ze-nickel zokushisa okuphezulu

Isengezo se-nickel sokushisa okuphezulu kokucwebezeliswa okuqhubekayo

Inombolo: I-Ni - 3000

instructions

NI-3000 iyisengezo esilungiselelwe ngokukhethekile sokucwecwa okuqhubekayo kwe-nickel sulfonate ku-substrate bese kuba msulwa (ekhanyayo/inkungu ) ithini. Lesi sengezo sivumela ucezu lokusebenza olupuletiwe ukuthi luphumelele izivivinyo zokugeleza kabusha kwezinga lokushisa eliphezulu (IR, ukugeleza kabusha) ngaphandle kokushintsha umbala kwendawo enamathelayo. Izici zayo eziyinhloko kanye nobuhle kufingqiwe kanje:

 ilungele ukusetshenziswa enkungu ye-sulfamic acid nickel base/sardines/bright tin process

 kulula ukuyisebenzisa, ingadluliswa Ukuhlaziywa kwe-titration elula

 ukusebenza kahle kwe-nickel ephezulu, ngaphandle kwesidingo sokushisa okuphezulu

 akuphazamisi ukusebenza kwe-nickel plating

 foam ephansi

 gcina ukushisela okuhle nokubukeka kwe-coating

Izimo zokusebenza:

Ni-3000 kufanele yengezwe enqubweni eqhubekayo ye-nickel sulfonate plating ekuhlanganiseni okungu-1% ngevolumu. Yonke eminye imingcele yokusebenza ye-nickel sulfamate ihlala ifana; Ukuze uthole amanye amapharamitha afanelekile, sicela ubhekisele kudatha yezobuchwepheshe efanele.

Ukwengezwa kwe-NI-3000 kuncike emiphumeleni yenqubo yokubhala titration enamathiselwe ngezansi. Inani elisetshenzisiwe lisekelwe ekuthathweni nasekusetshenzisweni kwe-plating. Inani elingeziwe lilinganiselwa ukuthi licishe libe ngu-0.5L/KAH, kodwa inani langempela eliyisengezo kufanele linqunywe ngokuya ngokusetshenziswa kwangempela.

Ukugxiliswa kwe-Ni-3000 kufanele kugcinwe phakathi kuka-5-20ml/L, kanye nenani elikhulu. kufanele kube ngu-10ml/L. Ukugxila kokusebenza okungaphansi kuka-5 mL/L kuzoholela ekwehleni kokusebenza (ithini lizoshintsha umbala ngemva kokuhlolwa kwezinga lokushisa eliphezulu).

Qaphela: i-NI-3000 inqubo ayikwazi ukusetshenziswa ngaphansi kwesimo sokugxila esingu-20ml/L

Uhlelo lokuhlaziya:

1.0 an ukubuka konke kwe-

1.1 Ukugxila kwesengezo se-Ni-3000 kusixazululo senqubo ye-nickel sulfonate kunganqunywa nge-iodometric titration nesisombululo se-sodium thiosulfate esingu-0.1N.

1.2 Inani elithile lesisombululo esijwayelekile/sokugeza siphawulwe ngenkomba yesitashi.

1.3 Ukugxila kwesithasiselo kubalwa ngenani elikhonjiswe ekuguqukeni ukusuka endaweni eluhlaza okwesibhakabhaka-onsomi ukuya endaweni yokugcina engenambala.

2.0 Izisetshenziswa kanye ne-Instruments

2.1 25 ml graduated cylinder

2.2 Amashubhu okuhlola angu-50ml amabili

2.3 Amabhodlela amabili e-iodine angu-250ml anezitobha

2.4 10ml pipette

3.0 Reagents and materials

3.1 reagent iodine ti1 0.

3.2 0.1N sodium thiosulfate reagent

3.3 isitashi inkomba (entsha)

3.4 Sodium bicarbonate

3 .5 i-glacial acetic acid

4.0 the program

4.1 Ngokusebenzisa isilinda sokulinganisa esingu-25ml, kala amanzi ahlanzekile angu-10ml ube yiflask ye-iodine engu-250ml bese uyimaka "engenalutho"

Utshwala obumhlophe ".

4.2 Sebenzisa i-pipette engu-20ml ukususa u-20.0ml wesisombululo esipholile sokusebenza ku-250ml

ibhodlela le-Iodine, bese ulebula "isixazululo sesampula".

4.3 Yengeza ngokucophelela cishe amagremu angu-2.5 e-sodium bicarbonate ebhodleleni ngalinye, ungawengezi kanye kanye

Kungenjalo , izokhipha ibhamuza ngokushesha. Govuza cishe iminithi elingu-1, i-sodium bicarbonate

Izoncibilika ngokuphelele.

4.4 Engeza u-40.0 mL we-0.1N isixazululo se-iodine ebhodleleni lesampula, xuba ngokushesha bese umisa ibhodlela. leave

Linganisa ivolumu ye-iodine engeziwe bese uyirekhoda njengokuthi V1

4.5 Engeza u-40.0 mL we-iodine engu-0.1N ebhodleleni elingenalutho bese ubhala ngokuthi V2

4.6 Beka womabili amabhodlela ebumnyameni ihora elilodwa ukuze vumela ukusabela okugcwele.

4.7 Ngemva kwehora elingu-1, ngeza kancane u-25 mL i-acetic acid ebhodleleni elibhalwe ukuthi "isixazululo sesampula". 0.1N i-sodium thiosulfate iye endaweni yokugcina engenambala.

4.9 Rekhoda umthamo we-0.1N sodium thiosulfate esetshenzisiwe -- V3.

4.10 Isixazululo esibhalwe ukuthi "blank" ebhodleleni, phinda u-4.6 kuya ku-4.8 bese urekhoda njenge-V4 .

5.0 calculation

Ukugxila kwe-Ni-3000 kubalwe kanje:

Ni - 3000 (ml/L) = {[(V1 (N1) (N2 (V3)]] - [((V2) (N1) (N2) (V4) x 50

-- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ----------------------------------------------------- -------------------------------------------------- ngo-41.15

Liquid sa mple quantity

Ivolumu esesinyathelweni 4.4 ithi V1

Ivolumu yesinyathelo 4.5 ithi V2

Ivolumu yesinyathelo 4.9 ingu-V3

Umthamo wesinyathelo 4.10 ngu-V4

I-concentration efanayo ye-iodine ngu-N1

Isilinganiso esilinganayo se-sodium thiosulfate ngu-N2

Iyunithi yevolumu yesixazululo sesampula ngu-ml

The equivalent concentration of sodium thiosulfate is N2

The volume unit of sample solution is ml