Plastic electroplating palladium activator
Plastic electroplating colloidal palladium activation inqubo (palladium water)
1. Uhlolojikelele
Amanzi e-Palladium iyi-acivator ene-acidic, exutshwe ne-hydrochloric acid . Yenzelwe i-plastic electroplating. Lesi sicuphi sizinze kakhulu futhi sinempilo ende yesevisi.
2. Izimo zokusebenza
Izinga lokushisa |
20℃-35℃ |
isikhathi |
1 kuya kumaminithi angu-5 |
concentration |
4-8 ml/litre |
I-asidi kasawoti |
2 5 0- 2 8 0ml /L |
Vuselela |
Kuyadingeka |
3.Izisetshenziswa
Trough |
Polyvinyl chloride, i-polypropylene, i-high density polypropylene, ingilazi noma ingilazi yePyrex |
Vuselela |
Ukugqugquzela umsebenzi noma ukujikeleza uketshezi lwethangi (nephampu), yenza ungasebenzisi umoya ukunyakazisa |
isihlungi |
---- ukuze ukhululeke ukusebenzisa okokusebenza kwe-polypropylene material |
Imishini yokukhipha umoya |
Kufanele ifakwe |
I-heater |
Uhlobo lwesemishi yamanzi ashisayo, i-quartz, i-Teflon |
4.Control and maintenance
Palladium water control range: 4-8 ml/litre
(A) ukulungiswa . 4 ml / l isixazululo esijwayelekile sokusebenza se-colorimetric
Thatha u-20 ml we-hydrochloric acid ehlanzekile ku-100 ml we-colorimetric tube wabe esengezwa u-0.4 mL wevolumu exutshwe namanzi e-palladium ku-100 ml , futhi unyakaziswa .
(B) yenziwe . 6 ml / l isixazululo esijwayelekile sokusebenza se-colorimetric
Thatha u-20 ml we-hydrochloric acid ehlanzekile ku-100 ml we-colorimetric tube wabe esengezwa u-0.6 mL wevolumu exutshwe namanzi e-palladium ku-100 ml , futhi unyakaziswa .
(C) ukwakheka . 8 ml / l isixazululo esijwayelekile sokusebenza se-colorimetric
Thatha u-20 ml we-analytical pure hydrochloric acid ku-100 ml colorimetric tube kwase kwengezwa u-0.8 mL wevolumu exutshwe ngamanzi e-palladium ku-100 ml , futhi unyakaziswa .
(D) I-concentration discovery
(1) thatha ngokuqondile uketshezi lwethangi bese uluthela eshubhuni elingenalutho le-colorimetric ukuze uqhathanise umbala nesixazululo esisebenzayo sombala esingenhla.
(2) Qhathanisa umbala nezixazululo ezihlukahlukene ezijwayelekile ukuze wahlulele I-palladium yamanzi ekhambi lokugeza elisebenzayo.
Uma kudingekile, engeza amanzi e-palladium ukuze ugcine ukugxila kwawo kuphakathi kuka-4-8 ml/litre.
Shintsha uketshezi olujwayelekile lombala masonto onke.
Uma ufuna ukuthola okwengeziwe imiphumela enembile, ungasebenzisa i-spectrophotometer, i-colorimeter, njll.
I-Divalent tin Ibanga lokulawula: 3.0-3.5 g/l
Uma kudingekile, engeza i-stannous chloride ukuze ulondoloze okuqukethwe kwe-divalent kuketshezi olusebenzayo phakathi kuka-3.0-3.5 g/l.
i-hydrochloric control range: 2. 5 0-2 . 8 0 ml / l
Indlela yokuhlaziya :
( 1 ) Sebenzisa ipayipi ukudonsa u-2 ml woketshezi lokugeza eflaskini ye-Erlenmeyer engu-250 ml.
( 2 ) Engeza cishe u-50 ml wamanzi ahlanzekile.
( 3 ) Engeza i-phenolic phenol indicator.
( 4 ) Kusixazululo se - sodium hydroxide esingu - 0.2N esifakwe endaweni ebomvu yokugcina .
Isibalo : I-Hydrochloric acid (ml/L ) = 41.44 × ukusetshenziswa kwe-sodium hydroxide (ml) × i-sodium hydroxide concentration (N)
Uma kudingeka, engeza i-hydrochloric acid ehlanzekile ukuze ugcine okuqukethwe kwe-hydrochloric acid esixazululweni esisebenzayo phakathi 250-280 ml/l
Ukungcola
Ukubekezelelwa koketshezi lokugeza ekungcoleni kokungcola yilokhu: Fe: <100ppm, Cr: <100ppm, nitrate nesibabule: <5ppm
iron ions, nitrate nesibabule: Ikakhulukazi isuselwa ku-hydrochloric acid engcolile, ezodala ukubola.
Chromium ion: Ikakhulukazi iphuma ekungangeni hlangothi okungaphelele, okuzoholela ekweqeni ukucwenga nokusetshenziswa okungavamile kwe-divalent tin.
Qaphela: Uma kungekho ukungcoliswa kokungcola, lokho ayidingi ukuqedwa futhi ingasetshenziswa ngokuqhubekayo, kodwa lapho izingxenye eziputshiwe ziwa, kufanele zicoshwe ngesikhathi.
5.Troubleshooting
Inkinga embi |
isizathu |
Countermeasure |
Ucwecwe oluqinile noma olugobile |
1. okugeza okulenga okuqinile . 2.I-divalent tin iphansi kakhulu . 3. Ukuwashwa okungalungile . |
1. Ukuhlunga okuzungezayo koketshezi lokugeza . 2. Khulisa i-divalent tin ibe ngu-3.0-3.5g/L. 3. Khulisa ukugeleza okuchichimayo kokuwasha, khulisa ukugezwa kwesifutho
|
Plating on hanger
|
Overactivation |
Yehlisa ukugxila noma izinga lokushisa kanye nesikhathi. |
Missing plating
|
Ukusebenza okunganele |
Khulisa izinga lokushisa noma ukugxilisa ingqondo, isikhathi . |
Ukubopha okungalungile
|
Ukwenza kusebenze okunganele |
Khulisa izinga lokushisa nokugxilisa ingqondo. |